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KMID : 0385520210340030128
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Analytical Science & Technology
2021 Volume.34 No. 3 p.128 ~ p.133
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Portable titrator equipped spectroscopic detectors; Spectrator
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Shin Ji-Won
Chae Gyo-Yoon
Kim Yea-Jin
Kim Sang-Ho
Chae Yoon-Su
Chae Won-Seok
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Abstract
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During titration, several chemical reactions result in changes not only in the potential of chemicals, but also in the colors of the indicator. In a potentiometric titration, a titration curve is obtained by measuring the abrupt change in the potential at the endpoint. Generally, acid?base titration is performed by observing the color change caused by an indicator to determine the endpoint. The method of determining the endpoint by measuring the potential difference has been well established and commercialized; however, the devices that can obtain the endpoint by observing the color change are limited. Consequently, in this study, a simple and precise spectral endpoint detector was manufactured using a drop-counter comprising an infrared emitter and a phototransistor, a white light LED as the light source and photodetector, and an analog-to-digital converter (Arduino). Spectrator, a new named, showed excellent results in terms of the reproducibility of acid?base titration using thymol blue as an indicator. Herein, we present the results of the Spectrator-manufacturing process as well as the experimental results.
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KEYWORD
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Titration, end-point, spectroscopic determination, portable titrator
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